A comment on my post on phosphorus oxychoride (which I still get hits on even now) from Andy Nation asked if there was any Org Syn prep or other respected documentation on the work-up or quench of this reagent.
The first source I thought of was the MSDS but it doesn’t really talk about quenching, just the hazards. And it is so vague that it is hardly useful for this point.
Secondly, I thought of Bretherick’s Handbook of Reactive Chemical Hazards.
Then I did a quick search and turned up a paper in Organic Process & Development which might tell you more than you want to know.
Any others out there?